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CUPEL

Volume 5 · 681 words · 1797 Edition

in metallurgy, a small vessel which absorbs metallic bodies when changed by fire into a fluid scoria; but retains them as long as they continue in their metallic state. One of the most proper materials for making a vessel of this kind is the ashes of animal bones; there is scarcely any other substance which so strongly resists vehement fire, which so readily imbibes metallic scoriae, and which is so little disposed to be vitrified by them. In want of these, some make use of vegetable ashes, freed by boiling in water from their saline matter, which would cause them melt in the fire.

The bones, burnt to perfect whiteness, so that no particle of coaly or inflammable matter may remain in them, and well washed from filth, are ground into moderately fine powder; which, in order to its being formed into cupels, is moistened with jut as much water as is sufficient to make it hold together when strongly pressed between the fingers; some direct glutinous liquids, as whites of eggs or gum-water, in order to give the powder a greater tenacity: but the inflammable matter, however small in quantity, which accompanies these fluids, and cannot be easily burnt out from the internal part of the mass, is apt to revive a part of the metallic scoria that has been absorbed, and to occasion the vessel to burst or crack. The cupel is formed in a brass ring, from three quarters of an inch to two inches diameter, and not quite so deep, placed upon some smooth support: the ring being filled with moistened powder, which is pressed close with the fingers; a round-faced pottle, called a monk, is struck down into it with a few blows of a mallet, by which the mass is made to cohere, and rendered sufficiently compact, and a shallow cavity formed in the middle: the figure of the cavity is nearly that of a sphere, that a small quantity of metal melted in it may run together into one bead. To make the cavity smoother, a little of the same kind of ashes levigated into an impalpable powder, and not moistened, is commonly sprinkled on the surface, through a small fine sieve made for this purpose, and the monk again struck down upon it. The ring or mould is a little narrower at bottom than at top; so that by pressing it down on some of the dry powder spread upon a table, the cupel is loosened, and forced upwards a little; after which it is easily pushed out with the finger, and is then set to dry in a warm place free from dust.

CUPPELLATION, the act of refining gold or silver by means of a cupel. For this purpose another vessel, called a muffle, is made use of, within which one or more cupels are placed. The muffle is placed upon a grate in a proper furnace, with its mouth facing the door, and as close to it as may be. The furnace being filled up with fuel, some lighted charcoal is thrown on the top, and what fuel is afterwards necessary is supplied through a door above. The cupels are let in the muffle; and being gradually heated by the successive kindling of the fuel, they are kept red-hot for some time, that the moisture which they strongly retain may be completely dissipated: for if any vapours should issue from them after the metal is put in, they would occasion it to sputter, and a part of it to be thrown off in little drops. In the sides of the muffle are some perpendicular slits, with a knob over the top of each, to prevent any small pieces of coals or ashes from falling in. The door, or some apertures made in it being kept open, for the inspection of the cupels, fresh air enters into the muffle, and passes off through these slits: by laying some burning charcoal on an iron plate before the door, the air is heated before its admission; and by removing the charcoal or supply- CUP